Triethylamine → HCID 178512739, compound

Participants

Reaction Steps

0.6 g (about 1.144 mmol) of the compound from Example 13A were dissolved in ml of ethanol, and 462 mg (4.574 mmol) of triethylamine and 71 mg (1.144 mmol) of hydrazine hydrate (80% strength solution in water) were added at 0° C. The mixture was stirred at RT overnight and then concentrated on a rotary evaporator. This gave 689 mg (purity about 60%) of the title compound.

Provenance & Evidence