Triethylamine → HCID 178512740, compound

Participants

Reaction Steps

0.62 g (0.901 mmol) of the compound from Example 9A (purity about 56%) were dissolved in 10.3 ml of ethanol, and 456 mg (4.506 mmol) of triethylamine and 70 mg (1.126 mmol) of hydrazine hydrate (80% strength solution in water) were added at 0° C. The mixture was stirred at RT overnight and then concentrated on a rotary evaporator. This gave a crude compound which was directly reacted further.

Provenance & Evidence