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HRID1529203

反应详情

EQUATION

反应方程式

HRID 1529203 的结构方程式

REACTANTS

反应物

2
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CNc1ccc(C#C[Si](C)(C)C)cn1
HCID66705950

未命名化合物

PRODUCTS

生成物

1
结构：C#Cc1ccc(NC)nc1
HCID22663128

5-Ethynyl-N-methylpyridin-2-amine

C8H8N2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The title compound is synthesized according to general procedure GP3 starting from 1.5 g (7.3 mmol) methyl-(5-trimethylsilanylethynyl-pyridin-2-yl)-amine (A6) and 507 mg (3.7 mmol) K2CO3 in 10 mL MeOH. Yield: 698 mg (56%) after chromatography on silica gel.