Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Succinimide | HCID 11439 | — |
| Reactant | Ethyl Nicotinate | HCID 69188 | — |
| Product | HCID 71001893 | HCID 71001893 | 5,075.4% |
Reaction Steps
Succinimide (2100 number average molecular weight, 368.8 g, 0.073 mol) and ethyl nicotinate (16.6 g, 0.11 mol) were charged to a 250 mL resin kettle equipped with an overhead stirrer, a Dean-Stark trap and a thermocouple. The reaction mixture was heated under a nitrogen atmosphere to 150° C. for 3 hours. The reaction mixture was diluted with 44.6 g process oil to afford 409.8 g of desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09090847B2 |
|---|
| Source dataset | uspto-grants-2015_07 |
|---|
| ORD ID | ord-35b2d011b5a041a4a4ee02ed976f662c |
|---|
| Source note | uspto-grants-2015_07 |
|---|
