HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178500968, compound → HCID 178500967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178500968 | HCID 178500968 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178500967 | HCID 178500967 | 96.9% |
Reaction Steps
23.0 g of dimethyl (cis-4-benzylaminocyclohexyl)malonate were dissolved in 200 ml of methanol and hydrogenated at 30 bar and 50° C. in the presence of 2 g of palladium catalyst (5% on carbon). Removal of the catalyst by filtration and subsequent concentration gave 16.0 g of the title product as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197729B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-50f383b40c404ce0b4640dcce518c620 |
| Source note | uspto-grants-2001_03 |