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HRID1531239

反应详情

EQUATION

反应方程式

HRID 1531239 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)NO
HCID98586

N-tert-Butylhydroxylamine

C4H11NO

结构：CC(C)(C)c1cc(C=O)c(O)c(C(C)(C)C)c1
HCID688023

3,5-Di-tert-butylsalicylaldehyde

C15H22O2

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc(C=[N+]([O-])C(C)(C)C)c(O)c(C(C)(C)C)c1
HCID178441041

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 1 using 3,5-di-tert-butyl-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 82.1% yield as a crystalline solid, m.p. 234.7-235.2° C. (Rf=0.66 on a silica gel plate using 1:4 EtOAc/hexanes as an eluant).

WORKUP

后处理

  1. customThe title compound was prepared