HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-tert-butylhydroxylamine → HCID 178441041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Reactant | 3,5-Di-tert-butylsalicylaldehyde | HCID 688023 | — |
| Product | HCID 178441041 | HCID 178441041 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1 using 3,5-di-tert-butyl-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 82.1% yield as a crystalline solid, m.p. 234.7-235.2° C. (Rf=0.66 on a silica gel plate using 1:4 EtOAc/hexanes as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197826B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-35a5fd3970a34d7c961f08a4925ace66 |
| Source note | uspto-grants-2001_03 |