HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-tert-butylhydroxylamine → HCID 178449916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Reactant | 3-Fluorosalicylaldehyde | HCID 587788 | — |
| Product | HCID 178449916 | HCID 178449916 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1 using 3-fluoro-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 92.7% yield as a yellow crystalline solid, m.p. 70.3° C. (Rf=0.25 on a silica gel plate using 7:3 hexanes/EtOAc as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197826B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-b624a19ca4144cbdbb4f1f90907f9131 |
| Source note | uspto-grants-2001_03 |