N-tert-butylhydroxylamine → HCID 178425260, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in Example 9 using 2-hydroxy-3-methylbenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 94% yield as a yellow crystalline solid, m.p. 59.2° C. (Rf=0.71 on a silica gel plate using 1:1 hexanes/EtOAc as an eluant).

Provenance & Evidence