2-Hydroxy-5-methoxybenzaldehyde → HCID 178492605, compound

HRID 1531243Notes

Reaction equation

HRID 1531243 reaction equation
[OH:1][C:2]1[CH:9]=[CH:8][C:7]([O:10][CH3:11])=[CH:6][C:3]=1[CH:4]=O.[C:12]([NH:16][OH:17])([CH3:15])([CH3:14])[CH3:13]>>[OH:1][C:2]1[CH:9]=[CH:8][C:7]([O:10][CH3:11])=[CH:6][C:3]=1[CH:4]=[N+:16]([C:12]([CH3:15])([CH3:14])[CH3:13])[O-:17]

Participants

3

Reactant 2

HCID 956952-Hydroxy-5-methoxybenzaldehydeHCID 98586N-tert-butylhydroxylamine

Product 1

HCID 178492605HCID 178492605, compound

Procedure

The title compound was prepared according to the procedure described in Example 1 using 2-hydroxy-5-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.1 % yield as a crystalline solid, m.p. 70.4-71.6° C. (Rf=0.23 on a silica gel plate using 3:7 EtOAc/hexanes as an eluant).

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-4a6cd4e28cc14f5a8ac5318cc3afab63
Source dataset
uspto-grants-2001_03
Patent number
US06197826B1

Reaction notes

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