HRID1531243

反应详情

EQUATION

反应方程式

HRID 1531243 的结构方程式

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 1 using 2-hydroxy-5-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.1 % yield as a crystalline solid, m.p. 70.4-71.6° C. (Rf=0.23 on a silica gel plate using 3:7 EtOAc/hexanes as an eluant).

WORKUP

后处理

  1. customThe title compound was prepared