化工社化工社 化学情報印刷レポート · 研究参考用
2-Hydroxy-5-methoxybenzaldehyde → HCID 178492605、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Hydroxy-5-methoxybenzaldehyde | HCID 95695 | — |
| 反応物 | N-tert-butylhydroxylamine | HCID 98586 | — |
| 生成物 | HCID 178492605 | HCID 178492605 | — |
反応手順
The title compound was prepared according to the procedure described in Example 1 using 2-hydroxy-5-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.1 % yield as a crystalline solid, m.p. 70.4-71.6° C. (Rf=0.23 on a silica gel plate using 3:7 EtOAc/hexanes as an eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06197826B1 |
| 出典データセット | uspto-grants-2001_03 |
| ORD ID | ord-4a6cd4e28cc14f5a8ac5318cc3afab63 |
| 出典メモ | uspto-grants-2001_03 |