HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Ethylvanillin → HCID 178466537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Ethylvanillin | HCID 68117 | — |
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Product | HCID 178466537 | HCID 178466537 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 13 using 3-ethoxy-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 36.4% yield as a yellow crystalline solid, m.p. 91.9° C. (Rf=0.25 on a silica gel plate using 1:1 EtOAc/hexanes as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197826B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-22c1535b0c694e0c8b939630a8b5d84a |
| Source note | uspto-grants-2001_03 |