2-Hydroxy-4-Methoxybenzaldehyde → HCID 178491266, compound

HRID 1531246Notes

Reaction equation

HRID 1531246 reaction equation
[OH:1][C:2]1[CH:9]=[C:8]([O:10][CH3:11])[CH:7]=[CH:6][C:3]=1[CH:4]=O.[C:12]([NH:16][OH:17])([CH3:15])([CH3:14])[CH3:13]>>[OH:1][C:2]1[CH:9]=[C:8]([O:10][CH3:11])[CH:7]=[CH:6][C:3]=1[CH:4]=[N+:16]([C:12]([CH3:15])([CH3:14])[CH3:13])[O-:17]

Participants

3

Reactant 2

HCID 696002-Hydroxy-4-MethoxybenzaldehydeHCID 98586N-tert-butylhydroxylamine

Product 1

HCID 178491266HCID 178491266, compound

Procedure

The title compound was prepared according to the procedure described in Example 1 using 2-hydroxy-4-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 72.9% yield as a pale yellow crystalline solid, m.p. 115.2-116.0° C. (Rf=0.49 on a silica gel plate using 1:1 EtOAc/hexanes as an eluant).

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-dfedbe3698be42c99b7d3e143a0f4d42
Source dataset
uspto-grants-2001_03
Patent number
US06197826B1

Reaction notes

Loading…