HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydroxy-4-Methoxybenzaldehyde → HCID 178491266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydroxy-4-Methoxybenzaldehyde | HCID 69600 | — |
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Product | HCID 178491266 | HCID 178491266 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1 using 2-hydroxy-4-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 72.9% yield as a pale yellow crystalline solid, m.p. 115.2-116.0° C. (Rf=0.49 on a silica gel plate using 1:1 EtOAc/hexanes as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197826B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-dfedbe3698be42c99b7d3e143a0f4d42 |
| Source note | uspto-grants-2001_03 |