HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,6-Dimethoxysalicylaldehyde → HCID 178493531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,6-Dimethoxysalicylaldehyde | HCID 69725 | — |
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Product | HCID 178493531 | HCID 178493531 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1 using 4,6-dimethoxy-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 60.7% yield as a yellow crystalline solid, m.p. 97.3° C. (Rf=0.38 on a silica gel plate using 7:3 hexanes/EtOAc as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197826B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-0715159da3fc4c86bc6daa5e69d04129 |
| Source note | uspto-grants-2001_03 |