HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-tert-butylhydroxylamine → HCID 178449925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Reactant | 2-Hydroxy-5-(trifluoromethoxy)benzaldehyde | HCID 1268058 | — |
| Product | HCID 178449925 | HCID 178449925 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1 using 2-hydroxy-5-trifluoromethoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 81.8% yield as a yellow crystalline solid, m.p. 82.6° C. (Rf=0.40 on a silica gel plate using 7:3 hexanes/EtOAc as an eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06197826B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-a79f332626924f2fa1e3b0a54fef58ad |
| Source note | uspto-grants-2001_03 |