HRID1531273

反应详情

EQUATION

反应方程式

HRID 1531273 的结构方程式

PROCEDURE

实验过程

The title compound is prepared as described for {5-[(4′-trifluoromethylbiphenyl-2-carbonyl)-amino]-indan-2-yl}-carbamic acid tert-butyl ester (the title E compound of Example 1) using N-(5-amino-indan-2-yl)-acetamide (the title A compound; 1.05 g, 5.50 mmol) and 2-bromo-benzoyl chloride (the title B compound; 1.21 g, 5.50 mmol) to give the product, mp 216-217° C. MS (ES+), m/z 373 (M+H), 375 (M+H).

WORKUP

后处理

  1. custom1.21 g, 5.50 mmol) to give the product, mp 216-217° C