Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1,2,3,4-Tetramethylcyclopentadiene | HCID 138163 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178426071 | HCID 178426071 | — |
Reaction Steps
Sodium hydride (containing mineral oil; the content of sodium hydride: 60%) (3.30 g) and aniline (0.237 g) were added to the solution of tetramethylcyclopentadiene (5.01 g) dissolved in tetrahydrofuran (45 ml), and stirred at 40° C. for 4 hours. Thus, tetramethylcyclopentadienylsodium was obtained in the form of a solution in tetrahydrofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06197990B1 |
|---|
| Source dataset | uspto-grants-2001_03 |
|---|
| ORD ID | ord-f1fa9962348e442994e43d9f880188b6 |
|---|
| Source note | uspto-grants-2001_03 |
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