Lauric Acid → HCID 14216684, compound

HRID 1531617Notes

Reaction equation

HRID 1531617 reaction equation
[O:1]=[CH:2][C@@H:3]([C@H:5]([C@@H:7]([C@@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4].[C:13](O)(=[O:25])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>CC(C)=O>[C:13]([O:1][CH2:2][C@@H:3]([OH:4])[C@@H:5]([OH:6])[C@H:7]([OH:8])[C@@H:9]([OH:10])[CH:11]=[O:12])(=[O:25])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

4

Reactant 2

HCID 3893Lauric AcidHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal

Product 1

HCID 14216684HCID 14216684, compoundYield 100.2%

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

2 ml of acetone were added to the reactor which contained 100 mg of Novozim 435, 60 mg of glucose and 200 mg of lauric acid. The reaction was carried out under mild continual agitation at 40° C. and water was continually removed from the reaction medium. 121 mg of glucose 6-monolaurate were obtained after 3 days of reaction corresponding to a yield of 99%.

Workup

  1. customwas carried out under mild continual agitation at 40° C.
  2. customwater was continually removed from the reaction medium

Sources & evidence

ORD record
ord-d58f9c5b7de64da4a30aa55a50ed5e09
Source dataset
uspto-grants-2001_03
Patent number
US06200784B1

Reaction notes

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