Lauric Acid → HCID 14216684, compound

HRID 1531618Notes

Reaction equation

HRID 1531618 reaction equation
[O:1]=[CH:2][C@@H:3]([C@H:5]([C@@H:7]([C@@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4].[C:13](O)(=[O:25])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>CC(C)=O>[C:13]([O:1][CH2:2][C@@H:3]([OH:4])[C@@H:5]([OH:6])[C@H:7]([OH:8])[C@@H:9]([OH:10])[CH:11]=[O:12])(=[O:25])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

4

Reactant 2

HCID 3893Lauric AcidHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal

Product 1

HCID 14216684HCID 14216684, compoundYield 98%

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

8 g of Novozim 435, 5 g of glucose and 16.7 g of lauric acid were added to 160 ml of acetone. After 5 days of mild agitation at 40° C. with constant removal of water from the reaction mixture, 9.6 g of glucose 6-monolaurate (98% yield) were obtained.

Workup

  1. customAfter 5 days of mild agitation at 40° C. with constant removal of water from the reaction mixture

Sources & evidence

ORD record
ord-8191f808fcc54b139254e83076b4f55d
Source dataset
uspto-grants-2001_03
Patent number
US06200784B1

Reaction notes

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