HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18326214, compound → HCID 21249837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18326214 | HCID 18326214 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21249837 | HCID 21249837 | — |
Reaction Steps
4-[methyl(phenylmethyl)amino]-6-[3-(trifluoromethyl) phenoxy] picolinic acid (0.42 g, 0.0010 mol) and a small amount of 10% palladium/carbon were added to about 30 ml of methanol. The obtained mixture was stirred at room temperature for about 10 hours in a hydrogen atmosphere. The obtained reaction solution was filtered using High-Flow Super Cell, and then concentrated, thereby obtaining an aimed product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200933B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-d663056d66e7478d811844901d442600 |
| Source note | uspto-grants-2001_03 |