HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4-Cyanophenylacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl (4-cyanophenyl)acetate | HCID 1512619 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Cyanophenylacetic acid | HCID 79587 | — |
Reaction Steps
14.2 g (0.081 mol) of methyl(4-cyano-phenyl)-acetate are dissolved in 100 ml ethanol and after the addition of 20 ml 2N sodium hydroxide solution stirred for 1 hour at ambient temperature. The solvent is distilled off, the residue is mixed with ice water and glacial acetic acid. The substance precipitated is suction filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200976B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-558571767c9f4bff80a036c8d6992d2a |
| Source note | uspto-grants-2001_03 |