Methylamine → 4-Bromo-N-methyl-2-nitroaniline

HRID 1531751Notes

Reaction equation

HRID 1531751 reaction equation

Br[C:2]1[CH:7]=[CH:6][C:5]([Br:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[CH3:12][NH2:13]>C(O)C>[Br:8][C:5]1[CH:6]=[CH:7][C:2]([NH:13][CH3:12])=[C:3]([N+:9]([O-:11])=[O:10])[CH:4]=1

Participants

4

Reactant 2

HCID 6329Methylamine

HCID 770041,4-Dibromo-2-nitrobenzene

Product 1

HCID 2580424-Bromo-N-methyl-2-nitroaniline

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 7a from 2,5-dibromo-nitrobenzene and methylamine solution in ethanol.

Sources & evidence

ORD record: ord-862a85c6b4d3420592be42f80fd2df79
Source dataset: uspto-grants-2001_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06200976B1

Reaction notes

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