HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylurea → HCID 21251008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylurea | HCID 6145 | — |
| Reactant | 1-Hexanol | HCID 8103 | — |
| Reactant | Cyclohexanone, 2-hydroxy- | HCID 10785 | — |
| Product | HCID 21251008 | HCID 21251008 | 29.6% |
Reaction Steps
A mixture of 4.5 g (39.4 mmol) of 2-hydroxycyclohexanone, 7.5 g (55 mmol) of phenylurea and 7 ml of hexanol is stirred under reflux for 20 hours. The mixture is concentrated under vacuum and the solid residue is recrystallized from acetone, and 2.5 g of product, m.p.=220° C., are recovered. Yield—29.6%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200991B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-97df9e49459e4439b29fe93617e7becd |
| Source note | uspto-grants-2001_03 |