HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 9954196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | HCID 131722425 | HCID 131722425 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9954196 | HCID 9954196 | — |
Reaction Steps
A mixture of the product from step (v) (0.175 g) and lithium hydroxide monohydrate (0.034 g) in tetrahydrofuran (3 ml) and water (3 ml) was stirred at room temperature for 3 hours and partitioned between dichloromethane and 2 M HCl. The organic phase was dried (MgSO4) and evaporated under reduced pressure. Yield 0.095 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200981B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-ba922c3c097e4e7cabd65ca863a55cca |
| Source note | uspto-grants-2001_03 |