2-Bromoethyl methyl ether → 3-[2-Methoxyethoxy]-5-[phenylmethoxy]benzoic acid, methyl ester

HRID 1531923Notes

Reaction equation

HRID 1531923 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([CH:9]=[C:10]([O:12][CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:11]=1)[C:5]([O:7][CH3:8])=[O:6].[CH3:20][O:21][CH2:22][CH2:23]Br>>[CH3:20][O:21][CH2:22][CH2:23][O:1][C:2]1[CH:3]=[C:4]([CH:9]=[C:10]([O:12][CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:11]=1)[C:5]([O:7][CH3:8])=[O:6]

Participants

3

Reactant 2

HCID 809722-Bromoethyl methyl etherHCID 7472028Methyl 3-(benzyloxy)-5-hydroxybenzoate

Product 1

HCID 1317224303-[2-Methoxyethoxy]-5-[phenylmethoxy]benzoic acid, methyl ester

Procedure

The subtitle compound was prepared from the product of step (i) (2.31 g) and 2-bromoethyl methyl ether 90.92 ml) by the method of example 11 step (i). Yield 2.74 g.

Sources & evidence

ORD record
ord-0c083dd64e6b439e933924e31f1de852
Source dataset
uspto-grants-2001_03
Patent number
US06200981B1

Reaction notes

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