HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[2-Methoxyethoxy]-5-[phenylmethoxy]benzoic acid, methyl ester → Methyl 3-hydroxy-5-(2-methoxyethoxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[2-Methoxyethoxy]-5-[phenylmethoxy]benzoic acid, methyl ester | HCID 131722430 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Methyl 3-hydroxy-5-(2-methoxyethoxy)benzoate | HCID 131722431 | — |
Reaction Steps
The product from step (ii) (2.74 g) was reduced by catalytic hydrogenation at 1 at. for 16 hours in ethyl acetate solution with 10% palladium on charcoal. Yield 1.5 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200981B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-da7f9a3430164230ae3e032e6eee9787 |
| Source note | uspto-grants-2001_03 |