Sulfuric Acid → HCID 60166995, compound

Participants

Reaction Steps

A solution of the product from step (i) (5.87 g) in acetic anhydride (4.32 g) was treated with concentrated sulphuric acid (0.5 ml) and stirred for 72 hours. The mixture was poured into ice-water and extracted with diethyl ether. The extract was washed with water and saturated aqueous sodium bicarbonate, dried (MgSO4) and evaporated. Yield 5.5 g.

Provenance & Evidence