HuagongsheHuagongshe Chemistry Print Report · For research reference only
M-Cresol → HCID 1540372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | M-Cresol | HCID 342 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 1540372 | HCID 1540372 | — |
Reaction Steps
A mixture of m-cresol (10.8 g), methyl bromoacetate (15.3 g) and potassium carbonate (69 g) in dimethylformamide (200 ml) was stirred overnight and partitioned between ethyl acetate and water. The organic phase was washed with water, dried (MgSO4) and evaporated. Purified by chromatography eluting with toluene. Yield 12.7 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200981B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-7ef21d5ce979415bbe40009b3a9574ba |
| Source note | uspto-grants-2001_03 |