Toluene → HCID 131722440, compound

Participants

Reaction Steps

A solution of the product of step (iii) (1.8 g) in trifluoroacetic acid (5 ml) and dichloromethane (30 ml) was stirred overnight at room temperature. Toluene was added and the mixture was evaporated. The residue was partitioned between ethyl acetate and saturated aqueous sodium bicarbonate. The organic phase was dried (MgSO4) and evaporated.

Provenance & Evidence