HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 131722445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | HCID 131722443 | HCID 131722443 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 131722445 | HCID 131722445 | — |
Reaction Steps
The product of step (v) (0.5 g) in tetrahydrofuran (20 ml) was treated with triphosgene (0.114 g) then pyridine (0.183 g). After 16 hours the reaction was evaporated and purified by chromatography eluting with 20% ethyl acetate in isohexane. Yield 0.4 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200981B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-502a3e1dbf1042e9a43c30916717f965 |
| Source note | uspto-grants-2001_03 |