Methyl bromoacetate → HCID 69693988, compound

HRID 1531944Notes

Reaction equation

HRID 1531944 reaction equation
[OH:1][C:2]1[CH:11]=[CH:10][CH:9]=[C:8]([OH:12])[C:3]=1[C:4]([O:6][CH3:7])=[O:5].Br[CH2:14][C:15]([O:17][CH3:18])=[O:16]>>[OH:1][C:2]1[CH:11]=[CH:10][CH:9]=[C:8]([O:12][CH2:14][C:15]([O:17][CH3:18])=[O:16])[C:3]=1[C:4]([O:6][CH3:7])=[O:5]

Participants

3

Reactant 2

HCID 60984Methyl bromoacetateHCID 519869Methyl 2,6-dihydroxybenzoate

Product 1

HCID 69693988HCID 69693988, compound

Procedure

The subtitle compound was prepared from the product of step (i) (10 g) and methyl bromacetate (5.5 ml) by the method of example 11 step (i). Purified by chromatography eluting with 20% ethyl acetate in isohexane. Yield 3.68 g.

Workup

  1. customPurified by chromatography
  2. washeluting with 20% ethyl acetate in isohexane

Sources & evidence

ORD record
ord-2df8a59fd83c40ad94a2956c95283296
Source dataset
uspto-grants-2001_03
Patent number
US06200981B1

Reaction notes

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