HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 131722450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 57033613 | HCID 57033613 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 131722450 | HCID 131722450 | — |
Reaction Steps
A mixture of the product from step (v) (0.46 g) and Lawesson's reagent (0.18 g) in benzene (5 ml) was heated at reflux for 2 hours. The mixture was evaporated and purified by chromatography eluting with 10% ethyl acetate in toluene. Yield 0.5 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06200981B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-5ba63cdc227c4409b8176d53dee2148d |
| Source note | uspto-grants-2001_03 |