HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dithiodibenzoic acid → 2,2'-Dithiobis[n-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamide]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dithiodibenzoic acid | HCID 8409 | — |
| Reactant | Tricyclo(3.3.1.13,7)dec-1-ylmethylamine | HCID 86625 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | 2,2'-Dithiobis[n-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamide] | HCID 88163524 | 30.6% |
Reaction Steps
Prepared according to the method of Example 14 from 1-adamantanemethylamine (0.23 g), 4-dimethylaminopyridine (0.006 g) and 2,2′dithiosalicylic acid (0.2 g) to give the sub-title compound as an off-white solid (0.12 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06201024B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-d8d5500e7c8c40b5914171d9f0187811 |
| Source note | uspto-grants-2001_03 |