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HRID1532308

反应详情

EQUATION

反应方程式

HRID 1532308 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccccc1SSc1ccccc1C(=O)O
HCID8409

Benzoic acid, 2,2'-dithiobis-

C14H10O4S2

结构：NCC12CC3CC(CC(C3)C1)C2
HCID86625

Tricyclo(3.3.1.13,7)dec-1-ylmethylamine

C11H19N

PRODUCTS

生成物

1
结构：O=C(NCC12CC3CC(CC(C3)C1)C2)c1ccccc1SSc1ccccc1C(=O)NCC12CC3CC(CC(C3)C1)C2
HCID88163524

未命名化合物

收率 30.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)c1ccncc1
催化剂HCID14284

N,N-Dimethylpyridin-4-amine

C7H10N2

PROCEDURE

实验过程

Prepared according to the method of Example 14 from 1-adamantanemethylamine (0.23 g), 4-dimethylaminopyridine (0.006 g) and 2,2′dithiosalicylic acid (0.2 g) to give the sub-title compound as an off-white solid (0.12 g).

WORKUP

后处理

  1. customPrepared