HCID 9801871, compound → HCID 9824989, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (0.13 ml) was added to a solution containing N,N-dimethyl-3-(2-pentadecyl-1H-benzimidazol-1-yl)-1-propanamine (0.20 g) in ethyl acetate (2 ml). After being stirred for 20 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethyl acetate-hexane, thereby yielding the entitled compound (0.13 g) as white solid.

Provenance & Evidence