HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9846158, compound → HCID 9869673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9846158 | HCID 9846158 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 9869673 | HCID 9869673 | — |
Reaction Steps
4N Hydrochloric acid/ethyl acetate solution (0.19 ml) was added to a solution containing 3-(2-heptadecyl-1H-benzimidazol-1-yl)-N,N-dimethyl-1-propanamine (0.33 g) in ethyl acetate (5 ml). After being stirred for 10 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (0.32 g) as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06204264B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-9200d9f4de064ba08d6153b591ed8acc |
| Source note | uspto-grants-2001_03 |