HCID 9845444, compound → HCID 9912263, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (0.12 ml) was added to a solution containing 2-(2-heptadecyl-1H-benzimidazol-1-yl)-N,N-dimethyl-1-ethanamine (0.200 g) in ethyl acetate (2 ml). After being stirred for 15 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethanol-ethyl acetate, thereby yielding the entitled compound (0.182 g) as white solid.

Provenance & Evidence