HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15869139, compound → 262357-39-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15869139 | HCID 15869139 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 262357-39-1 | HCID 22013745 | 99.7% |
Reaction Steps
10% of palladium-carbon (0.804 g) was added to a solution containing N-[3-(1H-imidazol-1-yl)propyl]-2-nitroaniline (4.000 g) in ethanol (40 ml) and stirred for 4.5 hours under a hydrogen gas atmosphere at room temperature. After the catalyst was removed out by filtration, the filtrate was concentrated, thereby yielding the entitled compound (3.503 g) as black solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06204264B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-80b278526eed4dfeba799c623ef56170 |
| Source note | uspto-grants-2001_03 |