HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3635836, compound → HCID 22013772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3635836 | HCID 3635836 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22013772 | HCID 22013772 | 72.3% |
Reaction Steps
10% of palladium-carbon (0.237 g) was added to a solution containing N-(3-morpholinopropyl)-2-nitroaniline (1.040 g) in ethanol (12 ml) and the mixture was stirred for 7 hours under a hydrogen gas atmosphere at room temperature. After the catalyst was removed out by filtration, the filtrate was concentrated, thereby yielding the entitled compound (0.667 g) as blackish brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06204264B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-1a6fd057d8774fbebee166422eacf186 |
| Source note | uspto-grants-2001_03 |