Acetate → HCID 9936216, compound

Participants

Reaction Steps

4N Hydrochloric acidlethyl acetate solution (0.24 ml) was added to a solution containing 3-(5-Chloro-2-heptadecyl-1H-benzimidazol-1-yl)-N,N-dimethyl-1-propanamine (0.46 g) in ethyl acetate (5 ml). After being stirred for 10 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethanol-ethyl acetate, thereby yielding the entitled compound (0.42 g) as white solid.

Provenance & Evidence