HCID 22013743, compound → 3-Amino-4-[[3-(dimethylamino)propyl]amino]-N-methylbenzamide

Participants

Reaction Steps

10% of palladium-carbon (0.40 g) was added to a solution containing 4-{[3-(dimethylamino)propyl]amino}-N-methyl-3-nitrobenzamide (1.88 g) in ethanol (30 ml) and the mixture was stirred for 14 hours under a hydrogen gas atmosphere at room temperature. After the catalyst was removed out by filtration, the filtrate was concentrated, thereby yielding the entitled compound (1.63 g) as purple solid.

Provenance & Evidence