HCID 22013755, compound → HCID 22013764, compound

Participants

Reaction Steps

10% of palladium-carbon (0.56 g) was added to a solution containing 4-{[3-(dimethylamino)propyl]amino}-N,N-dimethyl-3-nitrobenzamide (2.82 g) in ethanol (20 ml) and the mixture was stirred for 13 hours under a hydrogen gas atmosphere at room temperature. After the catalyst was removed out by filtration, the filtrate was concentrated, thereby yielding the entitled compound (2.59 g) as dark red solid.

Provenance & Evidence