HCID 9890245, compound → HCID 22013784, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (0.28 ml) was added to a solution containing 3-(2-heptadecyl-5-methyl-1H-benzimidazol-1-yl)-N,N-dimethyl-1-propanamine (0.34 g) in ethyl acetate (5 ml). After being stirred for 10 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with a mixed solution of ethanol-ethyl acetate, thereby yielding the entitled compound (0.304 g) as white solid.

Provenance & Evidence