HCID 9827780, compound → HCID 9827779, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (0.19 ml) was added to a solution containing 3-(7-chloro-2-heptadecyl-1H-benzimidazol-1-yl)-N,N-dimethyl-1-propanamine (0.363 g) in ethyl acetate (3 ml). After being stirred for 10 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with a mixed solution of ethanol-ethyl acetate, thereby yielding the entitled compound (0.284 g) as white solid.

Provenance & Evidence