HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22013766, compound → HCID 22013747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22013766 | HCID 22013766 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22013747 | HCID 22013747 | 99.1% |
Reaction Steps
10% of palladium-carbon (1.52 g) was added to a solution containing N-(2-nitrophenyl)-1-octadecanamine (7.600 g) in ethyl acetate (76 ml) and the mixture was stirred for 18 hours under a hydrogen gas atmosphere at room temperature. After the catalyst was removed out by filtration, the filtrate was concentrated, thereby yielding the entitled compound (6.95 g) as pink solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06204264B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-8ebecda9d7ba4cf2a751581e617e7d34 |
| Source note | uspto-grants-2001_03 |