Benzoyl chloride → HCID 22013744, compound

HRID 1532697Notes

Reaction equation

HRID 1532697 reaction equation
C(N(CC)CC)C.[CH3:8][N:9]([CH3:40])[CH2:10][CH2:11][CH2:12][N:13]1[C:17]2[CH:18]=[CH:19][C:20]([NH2:22])=[CH:21][C:16]=2[N:15]=[C:14]1[CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH3:39].[C:41](Cl)(=[O:48])[C:42]1[CH:47]=[CH:46][CH:45]=[CH:44][CH:43]=1>C(Cl)(Cl)Cl>[CH3:40][N:9]([CH3:8])[CH2:10][CH2:11][CH2:12][N:13]1[C:17]2[CH:18]=[CH:19][C:20]([NH:22][C:41](=[O:48])[C:42]3[CH:47]=[CH:46][CH:45]=[CH:44][CH:43]=3)=[CH:21][C:16]=2[N:15]=[C:14]1[CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH3:39]

Participants

5

Reactant 3

HCID 7412Benzoyl chlorideHCID 8471TriethylamineHCID 9955726HCID 9955726, compound

Product 1

HCID 22013744HCID 22013744, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Triethylamine is added to a solution containing Compound 27 in chloroform, and then benzoyl chloride is added thereto while being cooled with ice. The mixture is stirred at room temperature to give the entitled compound.

Workup

  1. temperaturewhile being cooled with ice
  2. customto give the entitled compound

Sources & evidence

ORD record
ord-54f7f824d29c4228a1ada5e5a9da0744
Source dataset
uspto-grants-2001_03
Patent number
US06204264B1

Reaction notes

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