HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 5-Chloro-2,2-dimethylpentanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 15688742 | HCID 15688742 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 5-Chloro-2,2-dimethylpentanoyl chloride | HCID 54487005 | — |
Reaction Steps
Oxalyl chloride (888 mg, 7 mmols) was added to a chloroform (10 ml) solution of the resulting carboxylic acid (0.9 g, 5 mmols) and DMF (catalytic amount, 1 drop), and stirred at room temperature for 1 hour. The reaction mixture was concentrated to obtain 5-chloro-2,2-dimethylpentanoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06204278B1 |
| Source dataset | uspto-grants-2001_03 |
| ORD ID | ord-67da03d656d64f06bcfb40b2f92742d8 |
| Source note | uspto-grants-2001_03 |