Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Heptanamine | HCID 8127 | — |
| Reactant | epsilon-CAPROLACTONE | HCID 10401 | — |
| Product | HCID 22633583 | HCID 22633583 | 78% |
Reaction Steps
A mixture of n-heptylamine (1.21 g, 10.5 mmols) and 6-hexanolactone (1.14 g, 10 mmols) was stirred at 100° C. for 3 hours, and then crystallized from ether-hexane to obtain 1.77 g (yield 78%) of N-heptyl-6-hydroxyhexaneamide as colorless crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06204278B1 |
|---|
| Source dataset | uspto-grants-2001_03 |
|---|
| ORD ID | ord-d545483b69654ad080f73b955994bb02 |
|---|
| Source note | uspto-grants-2001_03 |
|---|
