HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → Furo[2,3-c]pyridin-5-ylmethanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | HCID 57423120 | HCID 57423120 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Furo[2,3-c]pyridin-5-ylmethanol | HCID 22047174 | 90,3% |
Reaktionsschritte
[2-(Trimethylsilyl)furo[2,3-c]pyridin-5-yl]methyl acetate (1.3 g, 4.9 mmol) was dissolved in ethanol (50 ml) and treated with potassium carbonate (0.82 g, 5.9 mmol) and heated under reflux for 18 hrs. The mixture was evaporated to dryness and the residue partitioned between ethyl acetate and water. The organic layer was dried, filtered and evaporated to yield the title compound (0.66 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07732461B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-e4c3c14929d3481dbdf5fef4818b6d0b |
| Quellennotiz | uspto-grants-2010_06 |