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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 15329Erstellt: 25. Oktober 2026

Potassium Carbonate → Furo[2,3-c]pyridin-5-ylmethanol

https://huagongshe.com/reaction/15329

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium CarbonateHCID 11430—
EduktHCID 57423120HCID 57423120—
LösungsmittelEthanolHCID 702—
ProduktFuro[2,3-c]pyridin-5-ylmethanolHCID 2204717490,3%

Reaktionsschritte

[2-(Trimethylsilyl)furo[2,3-c]pyridin-5-yl]methyl acetate (1.3 g, 4.9 mmol) was dissolved in ethanol (50 ml) and treated with potassium carbonate (0.82 g, 5.9 mmol) and heated under reflux for 18 hrs. The mixture was evaporated to dryness and the residue partitioned between ethyl acetate and water. The organic layer was dried, filtered and evaporated to yield the title compound (0.66 g).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07732461B2
Quelldatensatzuspto-grants-2010_06
ORD IDord-e4c3c14929d3481dbdf5fef4818b6d0b
Quellennotizuspto-grants-2010_06